Beale, T.A.W. and Hase, T.P.A. and Iida, T. and Endo, K. and Steadman, P. and Marshall, A.R. and Dhesi, S.S. and van der Laan, G. and Hatton, P.D. (2010) 'RASOR : an advanced instrument for soft x-ray reflectivity and diffraction.', Review of scientific instruments., 81 (7). 073904.
We report the design and construction of a novel soft x-ray diffractometer installed at Diamond Light Source. The beamline endstation RASOR is constructed for general users and designed primarily for the study of single crystal diffraction and thin film reflectivity. The instrument is comprised of a limited three circle (θ, 2θ, and χ) diffractometer with an additional removable rotation (ϕ) stage. It is equipped with a liquid helium cryostat, and post-scatter polarization analysis. Motorized motions are provided for the precise positioning of the sample onto the diffractometer center of rotation, and for positioning the center of rotation onto the x-ray beam. The functions of the instrument have been tested at Diamond Light Source, and initial test measurements are provided, demonstrating the potential of the instrument.
|Keywords:||Cryostats, X-ray diffractometeres, X-ray reflection, Resonant magnetic scattering, Active pixel sensor, Exchange Scattering, Bragg-diffractio, Multilayers, Anisotropy, Edges, Films, Iron.|
|Full text:||PDF - Published Version (1214Kb)|
|Publisher Web site:||http://dx.doi.org/10.1063/1.3458004|
|Publisher statement:||Copyright 2010 American Institute of Physics. This article may be downloaded for personal use only. Any other use requires prior permission of the author and the American Institute of Physics. The following article appeared in Beale, T.A.W. and Hase, T.P.A. and Iida, T. and Endo, K. and Steadman, P. and Marshall, A.R. and Dhesi, S.S. and van der Laan, G. and Hatton, P.D. (2010) 'RASOR : an advanced instrument for soft x-ray reflectivity and diffraction.', Review of scientific instruments., 81 (7). 073904 and may be found at http://dx.doi.org/10.1063/1.3458004|
|Record Created:||09 Oct 2012 10:35|
|Last Modified:||05 Aug 2014 11:20|
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