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Preparation and complete 1 H and 13C assignment of some pentacyclo [5.4.0.02,6.03,10.05,9]undecane-8,11-dione (PCUD) derivatives

Kenwright, Alan M.; Sellars, Jonathan D.

Preparation and complete 1 H and 13C assignment of some pentacyclo [5.4.0.02,6.03,10.05,9]undecane-8,11-dione (PCUD) derivatives Thumbnail


Authors

Alan M. Kenwright

Jonathan D. Sellars



Abstract

The preparation of a number of alkyl and alkoxy derivatives of pentacyclo[5.4.0.02,6.03,10.05,9]undecane-8,11-dione derivatives utilising a cheap, practical, low energy, ‘green’, single-pass continuous flow photochemical reactor is reported. Their 1 H and 13C NMR spectra are fully assigned, revealing some general characteristics not previously reported for this class of compound, which should aid the assignment and prediction of the NMR spectra of PCUD derivatives.

Citation

Kenwright, A. M., & Sellars, J. D. (2012). Preparation and complete 1 H and 13C assignment of some pentacyclo [5.4.0.02,6.03,10.05,9]undecane-8,11-dione (PCUD) derivatives. Magnetic Resonance in Chemistry, 50(12), 803-808. https://doi.org/10.1002/mrc.3879

Journal Article Type Article
Publication Date Dec 1, 2012
Deposit Date Nov 19, 2014
Publicly Available Date Mar 28, 2024
Journal Magnetic Resonance in Chemistry
Print ISSN 0749-1581
Electronic ISSN 1097-458X
Publisher Wiley
Peer Reviewed Peer Reviewed
Volume 50
Issue 12
Pages 803-808
DOI https://doi.org/10.1002/mrc.3879

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Copyright Statement
This is the accepted version of the following article: Kenwright, A. M. and Sellars, J. D. (2012), Preparation and complete 1 H and 13C assignment of some pentacyclo[5.4.0.02,6.03,10.05,9]undecane-8,11-dione (PCUD) derivatives. Magnetic Resonance in Chemistry, 50 (12): 803–808, which has been published in final form at http://dx.doi.org/10.1002/mrc.3879. This article may be used for non-commercial purposes in accordance With Wiley Terms and Conditions for self-archiving.




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