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Versatile, Cheap, Readily Modifiable Sample Delivery Method for Analysis of Air-/Moisture-Sensitive Samples Using Atmospheric Pressure Solids Analysis Probe Mass Spectrometry

Strong, Kerry A.; Stokes, Peter; Parker, David; Buckley, Amy K.; Mosely, Jackie A.; Brodie, Claire N.; Dyer, Philip W.

Versatile, Cheap, Readily Modifiable Sample Delivery Method for Analysis of Air-/Moisture-Sensitive Samples Using Atmospheric Pressure Solids Analysis Probe Mass Spectrometry Thumbnail


Authors

Kerry Strong k.a.strong@durham.ac.uk
Senior Technician (Biomarkers)

Peter Stokes peter.stokes@durham.ac.uk
Mass Spectrometry Service Manager

Amy K. Buckley

Jackie A. Mosely

Claire N. Brodie



Abstract

A cheap, versatile, readily modified, and reusable glass probe system enabling delivery of solid air-/moisture-sensitive samples for mass spectrometric (MS) analysis using an Atmospheric pressure Solids Analysis Probe (ASAP) is described. The simplicity of the design allows quick and easy ASAP MS analyses of sensitive solid and liquid samples without the need for any modifications to commercially available vertically loaded ASAP mass spectrometers. A comparison of ASAP mass spectra obtained for metal complexes under air and an inert atmosphere is given.

Citation

Strong, K. A., Stokes, P., Parker, D., Buckley, A. K., Mosely, J. A., Brodie, C. N., & Dyer, P. W. (2022). Versatile, Cheap, Readily Modifiable Sample Delivery Method for Analysis of Air-/Moisture-Sensitive Samples Using Atmospheric Pressure Solids Analysis Probe Mass Spectrometry. Analytical Chemistry, 94(32), 11315-11320. https://doi.org/10.1021/acs.analchem.2c02039

Journal Article Type Article
Acceptance Date Jul 22, 2022
Online Publication Date Aug 5, 2022
Publication Date 2022
Deposit Date Aug 19, 2022
Publicly Available Date Mar 29, 2024
Journal Analytical Chemistry
Print ISSN 0003-2700
Electronic ISSN 1520-6882
Publisher American Chemical Society
Peer Reviewed Peer Reviewed
Volume 94
Issue 32
Pages 11315-11320
DOI https://doi.org/10.1021/acs.analchem.2c02039

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