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Conserved hydrogen bonding in tetrahydrocarbazolone derivatives : influence of solution-state assembly on crystal form nucleation.

Edkins, Robert M. and Hayden, Elliott and Steed, Jonathan W. and Fucke, Katharina (2015) 'Conserved hydrogen bonding in tetrahydrocarbazolone derivatives : influence of solution-state assembly on crystal form nucleation.', Chemical communications., 51 (25). pp. 5314-5317.

Abstract

Two tetrahydocarbazolone derivatives were found to show multiple unsolvated crystal forms. A persistent dimer motif was detected in solution by FTIR spectroscopy that is maintained in the kinetic crystal forms. Rationally introduced steric bulk induces the formation of a more stable catemeric form.

Item Type:Article
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Status:Peer-reviewed
Publisher Web site:http://dx.doi.org/10.1039/C4CC10453F
Publisher statement:This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
Date accepted:10 February 2015
Date deposited:09 March 2015
Date of first online publication:March 2015
Date first made open access:No date available

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