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Versatile, Cheap, Readily Modifiable Sample Delivery Method for Analysis of Air-/Moisture-Sensitive Samples Using Atmospheric Pressure Solids Analysis Probe Mass Spectrometry

Strong, Kerry A. and Stokes, Peter and Parker, David and Buckley, Amy K. and Mosely, Jackie A. and Brodie, Claire N. and Dyer, Philip W. (2022) 'Versatile, Cheap, Readily Modifiable Sample Delivery Method for Analysis of Air-/Moisture-Sensitive Samples Using Atmospheric Pressure Solids Analysis Probe Mass Spectrometry.', Analytical Chemistry, 94 (32). pp. 11315-11320.

Abstract

A cheap, versatile, readily modified, and reusable glass probe system enabling delivery of solid air-/moisture-sensitive samples for mass spectrometric (MS) analysis using an Atmospheric pressure Solids Analysis Probe (ASAP) is described. The simplicity of the design allows quick and easy ASAP MS analyses of sensitive solid and liquid samples without the need for any modifications to commercially available vertically loaded ASAP mass spectrometers. A comparison of ASAP mass spectra obtained for metal complexes under air and an inert atmosphere is given.

Item Type:Article
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Status:Peer-reviewed
Publisher Web site:https://doi.org/10.1021/acs.analchem.2c02039
Publisher statement:© 2022 The Authors. Published by American Chemical Society. This is an open access article under the CC BY license (https://creativecommons.org/licenses/by/4.0/)
Date accepted:22 July 2022
Date deposited:19 August 2022
Date of first online publication:05 August 2022
Date first made open access:19 August 2022

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